표제지
목차
Abstract 8
서론 10
재료 및 방법 12
1. 재료 12
2. 시약 및 표준품 12
3. 잔류농약 분석방법 16
3-1. 추출 및 농축 16
3-2. 정제 16
3-3. 기기분석 17
결과 및 고찰 21
1. 검출농약의 잔류 특성 21
1-1. 회수율 및 검출 한계 21
1-2. 품목별 잔류농약 검출률 23
1-3. 품목별 잔류농약 종류 및 특성 27
1-4. 농약성분별 잔류농약 분석결과 33
2. 과일별 검출농약의 인체 위해성 평가 39
요약 47
참고문헌 49
Appendix 55
Table 1. The list of sample collected and analyzed 13
Table 2. Pesticides for GC/MS/MS analysis 14
Table 3. GC/MS/MS conditions used in the determination of... 19
Table 4. MRM transition for the pesticide in the analytical conditions 20
Table 5. Recovery rate, % RSD, LOD and LOQ of pesticides detected 22
Table 6. Analyzed sample numbers and detection rate of... 25
Table 7. Concentration of residual pesticides from detected samples 30
Table 8. Numbers of samples detection on origin 32
Table 9. Detected pesticides and commo dities 35
Table 10. Comparison of fruits intakes in Korea 42
Table 11. ADI values used for the chronic risk assessment 43
Table 12. Body weights of people according to gender and age in Korea 44
Table 13. Risk assessment of pesticides detected from imported fruits 45
Fig. 1. Analyzed sample numbers and numbers of detection... 26
Fig. 2. Numbers of samples with detections. 28
Fig. 3. Percentage of pesticides detected by use. 34
Fig. 4. Frequency and detection rate of pesticide residues... 36