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Title page
Abstract
국문요약
Contents
Chapter 1 Introduction 16
1.1. Electrophoretic Display 17
1.2. Electronic ink particles 18
1.2.1. Hollow inorganic nanoparticles as electronic inks 18
1.2.2. Polymeric colored electrophoretic nanoparticles 21
1.3. References 24
Chapter 2 Preparation and Characterization of Monodisperse Polymer Nanoparticles of Various Size via Emulsifier-free Emulsion Polymerization 26
2.1. Introduction 27
2.2. Experimental 30
2.2.1. Chemicals 30
2.2.2. Syntheses 30
2.2.3. Characterizations 31
2.3. Results and Discussion 32
2.4. Conclusions 40
2.5. References 41
Chapter 3 Synthesis of Monodisperse Hollow Titania Nanospheres Using a Cationic Colloidal Template 43
3.1. Introduction 44
3.2. Experimental 47
3.2.1. Materials 47
3.2.2. Preparation of Hollow Titania Nanospheres 47
3.2.3. Characterization 48
3.3. Results and Discussion 51
3.4. Conclusions 65
3.5. References 66
Chapter 4 Preparation and Characterization of Colored Electronic Ink Particles by High Temperature-Assisted Dyeing for Electrophoretic Displays 69
4.1. Introduction 70
4.2. Experimental 72
4.2.1. Materials 72
4.2.2. Emulsifier-Free Emulsion Polymerization 72
4.2.3. Surface Modification of PMMA Particles by Aminolysis 73
4.2.4. Disperse Dyeing of NH2-PMMA Particles 73
4.2.5. Characterization 74
4.3. Results and Discussion 75
4.3.1. Emulsifier-free Emulsion Copolymerizations 75
4.3.2. Aminolysis 76
4.3.3. Disperse dyeing 77
4.3.4. Electrphoretic Mobility 79
4.4. Conclusions 89
4.5. References 90
Table 2.1. Polymer Nanospheres Prepared at Various Reaction Conditions 35
Table 4.1. Zeta Potential analysis of nanoparticles. 80
Figure 1.1. The microcapsulated electrophoretic display. 18
Figure 1.2. Schematic illustration of the he layer-by-layer (LbL) self-assembly process for forming polyelectrolyte multilayers on particles. 20
Figure 1.3. Schematic diagram of the formation procedure of PSA/silver core-shell particles and silver/TiO₂ hollow spheres. 21
Figure 2.1. Chemical structure of ater-soluble cationic comonomer MOTAC (I) and initiator (II). 36
Figure 2.2. Schematic showing particle-formation mechamism. 37
Figure 2.3. SEM images and size distribution of the cationic PS nanoparticles, prepared with various monomer concentrations. 38
Figure 2.4. Particle size distribution of polymer nanospheres as a template (C2). 39
Figure 3.1. TEM(a) and SEM(b) images of titania-coated polymer nanospheres. 59
Figure 3.2. TEM(a) and SEM(b) images of hollow titania nanospheres. 60
Figure 3.3. wide-angle XRD patterns of titania-coated polymer particles(a) and hollow titania particles. 61
Figure 3.4. SAXS analysis of template polymer nanospheres(C2)(a), titania-coated polymer nanoapheres(b) and hollow titania nanoapheres(c). 62
Figure 3.5. Comparison of FTIR spectra of polymer nanospheres(C2)(a), titania-coated polymer nanoapheres(b) and hollow titania nanoapheres(c). 63
Figure 3.6. TGA data of titania-coated and uncoated nanoparticles. 64
Figure 4.1. Chemical structure of the disperse dyes used in the present study. 81
Figure 4.2. Schematic presentation of the preparation of cross-linked PMMA nanoparticles. 82
Figure 4.3. Size distribution of PMMA nanoparticles with various MOTAC concentration. 83
Figure 4.4. DSC data of cross-linked PMMA nanoparticles (a, 170 nm). 84
Figure 4.5. Method for surface modification by aminolysis. 85
Figure 4.6. FTIR spectra of unmodified PMMA particles (a) and amine modified PMMA particles (b). 86
Figure 4.7. SEM images and photograph of dyed PMMA nanoparticles by C.I. disperse red 152 (a), C.I. disperse yellow 241 (b) and C.I. disperse blue 73 (c). 87
Figure 4.8. Absorption spectra of disperse dyes in colored particles. 88
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